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ASTM E1967-1998(2003) 用油浸法和相衬显微镜自动测定玻璃样品的折射指数的标准试验方法

作者:标准资料网 时间:2024-05-19 21:33:53  浏览:9024   来源:标准资料网
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【英文标准名称】:StandardTestMethodfortheAutomatedDeterminatonofRefractiveIndexofGlassSamplesUsingtheOilImmersionMethodandaPhaseContrastMicroscope
【原文标准名称】:用油浸法和相衬显微镜自动测定玻璃样品的折射指数的标准试验方法
【标准号】:ASTME1967-1998(2003)
【标准状态】:现行
【国别】:
【发布日期】:1998
【实施或试行日期】:
【发布单位】:美国材料与试验协会(US-ASTM)
【起草单位】:E30.01
【标准类型】:(TestMethod)
【标准水平】:()
【中文主题词】:折射指数;玻璃比对;玻璃测量
【英文主题词】:glasscomparisions;glassmeasurement;refractiveindex
【摘要】:Thistechniquemodifiesthesample,inthattheglassfragmentmustbecrushed,ifitistoolarge,andimmersedinoilfortheanalysis.Somesamplehandling,however,wouldenabletheanalysttorecoverthesampleinthecrushedform,ifnecessary.Thistestmethodisusefulforaccuratemeasurementofx03B7;Dtfromawidevarietyofglasssamples,wheremostglassesofinteresthavex03B7;Dtintherangebetween1.48x2013;1.55inx03B7;Dtunits.Theobjectivenatureofthematchpointdeterminationallowsforabetterstandardizationbetweenlaboratories,andtherefore,allowsfortheinterchangeofdatabasesbetweenlaboratories.Itshouldberecognizedthatsurfacefragments,especiallyfromfloatglasssamples,canresultinx03B7;Dt,smeasurablyhigherthanfragmentsfromthebulkofthesamesource(5).Theprecisionandbiasofthistestmethodshouldbeestablishedineachlaboratorythatemploysit.Confidenceintervalsorasimilarstatisticalqualitystatementshouldbequotedalongwithanyreportedx03B7;Dtvalue.Forinstance,alaboratorymayreportthattheerrorforthemeasurement,usingareferenceopticalglassis0.00003units.Itshouldberecognizedthatthistechniquemeasurestherefractiveindexoftheglassatthematchpointtemperature,whichwillbehigherthanambienttemperature,andthus,maygivedifferentx03B7;Dtvaluesfromthoseobtainedbyothermethods,whichmeasuretherefractiveindexatroomtemperature.1.1Thistestmethodcoversaprocedureformeasuringtherefractiveindex(951;955;t)ofglasssamples,irregularlyshapedandassmallas300956;g,forthecomparisonoffragmentsofaknownsourcetorecoveredfragmentsfromaquestionedsource.1.2Thistestmethoddoesnotincludethemeasurementofopticaldispersionorthemeasurementofrefractiveindex(951;955;t)atanyotherwavelengthotherthantheSodiumDline(951;Dt).Thismethodemploysanarrowbandpassfilterat589nm,butotherfilterscouldbeemployedusingthedescribedmethodandallowingthe951;955;ttobedeterminedatotherwavelengths,therefore,alsoallowingforthedispersionvaluetobecalculated.1.3Alternativemethodsforthedeterminationof951;955;tarelistedinRefs(1-5).1.4Thisstandardtestmethoddoesnotpurporttoaddressallofthesafetyconcerns,ifany,associatedwithitsuse.Itistheresponsibilityoftheusertoestablishappropriatesafetyandhealthpracticesanddeterminetheapplicabilityofregulatorylimitationspriortouse.
【中国标准分类号】:N32
【国际标准分类号】:81_040_01
【页数】:3P.;A4
【正文语种】:


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MIL-H-8775D (AMENDMENT 1), MILITARY SPECIFICATION: HYDRAULIC SYSTEM COMPONENTS, AIRCRAFT AND MISSILES, GENERAL SPECIFICATION FOR (28 JUL 1976) [S/S BY SAE-AS8775].

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